Preparation and standardization of 0.1M Perchloric acid solution

Preparation and standardization of 0.1M Perchloric acid solution   1. Preparation: Mix 8.5ml of Perchloric acid with 500ml of anhydrous glacial acetic acid & 25ml of acetic anhydride, cool and add anhydrous glacial acetic acid to produce 1000ml, allow the prepared solution to stand for one day for the excess acetic anhydride to be combined … Read more