Analysis method of Enrofloxacin Suspension
1.1 To lay down a procedure for analysis of Enrofloxacin Suspension.
2.1 This procedure is applicable to the analysis of Enrofloxacin Suspension. quality control laboratories
3.1 Q.C- Chemist
4.1 Manager-Quality Assurance
5.1 Description: Pour 50ml finish sample in beaker and observed visually.
5.2 pH: Taken 50 ml sample in beaker rinse the pH electrode first with purified water followed by sample dip the electrode in sample and observed the pH.
5.3 Volume variation: Measured the volume by measuring cylinder and determine the volume variation.
5.4.1 In the assay, the principle peak in the chromatogram obtain with the test solution correspond to the peak in the chromatogram obtained with the reference solution.
Each 1.0 ml contains:
Enrofloxacin IP 100mg.
Estimation of Enrofloxacin suspension:
Method of Enrofloxacin suspension:
Method: BY HPLC
Mobile phase: Phosphoric acid : Acetonitrile
85 : 15
Standard preparation: Weight 100 mg of Enrofloxacin diluted to 100 ml volumetric flask with Mobile phase.
Sample preparation: Weight accurately equivalent to 100 mg. Enrofloxacin diluted to 100 ml volumetric flask volumetric flask with Mobile phase.
Flow rate – 1.0 ml /mint.
column -C18 (150mm x4.6) 5µm.
Injection Volume -20µl.
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|1.0||STP||Standard Testing Procedure.|
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